Sample Extraction Needle
NeedlEx

Sample Extraction Needle

 
Features of NeedlEx
 
NeedlEx enables easy extractions of samples and provides superior reproducibility.

By attaching a NeedlEx needle to a gas sampler and simply aspirating a sample, the desired sample can be extracted selectively and accurately concentrated in a very short period of time.

Adsorbed samples can be stored in NeedlEx needles.

Extracted samples can be stored for approximately ten days by sealing both ends of NeedlEx needles using Teflon plugs included with each needle.

No additional equipment is required for the adsorption and desorption of samples.

Desorption of samples is performed using the heat produced by gas chromatograph injection ports. Extracted samples can be injected into GCs using gas tight syringes and 1 mL of N2.

NeedlEx needles can be used repeatedly.

By conditioning NeedlEx needles in GC injection ports for 3 minutes after each analysis, needles can be used approximately 25 to 30 times.



NeedlEx Types
For organic solvents

Extractions of general organic solvents including ethyl acetate, isobutanol, methyl isobutyl ketone, toluene, xylene, and styrene, etc.

For trimethylamine

Extractions of short chain amines including trimethylamine, etc.

For fatty acids

Extractions of fatty acids (propionic acid, isobutyric acid, n-butyric acid, isovaleric acid).

For petroleum products

Identifications of trace amounts of petroleum products.




NeedlEx Specifications
Inner diameter: 0.5 mm
Outer diameter: 0.7 mm
Length: 85 mm Luer lock type needle with side hole



NeedlEx Measurement Ranges (Sample concentrations and sampling volumes)
1) Organic solvent type

Breakthrough volumes depend on the type of solvent being measured. When the concentration of an organic solvent in air is less than or equal to 100 ng/mL (and for samples with multiple constituents each with a concentration less than or equal to 100 ng/mL), please refer to the sampling volume table shown below.

 
Sampling volume Sample
10 mL Acetone, chloroform, cis-dichloroethylene, 1,2-dichloroethane, ethanol, methyl acetate, 2-propanol, tetrachloromethane, tetrahydrofuran, 1,1,1-trichloroethane, trichloroethylene
50 mL

Ethyl acetate, isopropyl acetate, methyl ethyl ketone

100 mL

n-Amyl acetate, 1-butanol, 2-butanol, n-butyl acetate, butyl cellosolve, chlorobenzene, cyclohexanol, cyclohexanone, dichlorobenzene, N,N-dimethylformamide, 1,4-dioxane, ethylbenzene, ethyl cellosolve, isoamyl acetate, isoamyl alcohol, isobutanol, isobutyl acetate, methyl cellosolve, n-propyl acetate, methyl n-butyl ketone, methylcyclohexanol, methylcyclohexanone, methyl isobutyl ketone, styrene, 1,1,2,2-tetrachloroethane, tetrachloroethylene, toluene, xylene

 *This product cannot be used for sampling of the low boiling point compounds methanol, dichloromethane, and diethyl ether. Please contact us for details regarding other gases.

2) Trimethylamine type

Trimethylamine can be extracted up to an absolute value of 200 ng.

3) Fatty acid type

Propionic, isobutyric, n-butyric, and isovaleric acid can each be extracted up to an absolute value of 10 ug.

4)

Petroleum product type

Up to 100 mL of gasoline vapor and up to 200 mL of each of kerosene and diesel vapor can be sampled.

Disposal of NeedlEx extraction needles

When disposing of NeedlEx extraction needles, separate and dispose of needle parts according to the type of material each part is made from. As NeedlEx needles are a potential source of injuries, place used needles in an appropriate metal container, and dispose of as waste metal.

Contact details for purchases
Application Chromatograms

Organic solvent type
Standard organic solvents
(20 mL sample)

Trimethylamine type

Trimethylamine in head space gas
of dry chicken manure

(100 mL sample)

Fatty acid type

Fatty acids in head space gas of shoes
(300 mL sample)

Petroleum product type

Gasoline  0.1 uL/L in N2
   (100 mL sample)
Column: ULBON HR-1
              30 m x 0.32 mm I.D. Df: 0.25
μm 
Column temp.: 50 (2 min hold)250,
               Program rate 10
/min
Split ratio: 10:1
Injection : 1 mL (280)
Detector: FID (250)
Carrier gas: He 1.7 mL/min 
Kerosene  0.1 uL/L in N2
(100 mL sample)
Column: ULBON HR-1
              30 m x 0.32 mm I.D. Df: 0.25
μm 
Column temp.: 50 (2 min hold)250,
               Program rate 10
/min
Split ratio: 10:1
Injection : 1 mL (280)
Detector: FID (250)
Carrier gas: He 1.7 mL/min 
Light oil  0.1 uL/L in N2
(100 mL sample)
Column: ULBON HR-1
              30 m x 0.32 mm I.D. Df: 0.25
μm 
Column temp.: 50 (2 min hold)250,
               Program rate 10
/min
Split ratio: 10:1
Injection : 1 mL (280)
Detector: FID (250)
Carrier gas: He 1.7 mL/min 
Mixture (gasoline, kerosene) 0.1 uL/L in N2
(100 mL sample)
Column: ULBON HR-1
              30 m x 0.32 mm I.D. Df: 0.25
μm 
Column temp.: 50 (2 min hold)250,
               Program rate 10
/min
Split ratio: 10:1
Injection : 1 mL (280)
Detector: FID (250)
Carrier gas: He 1.7 mL/min